The synthesis of a novel DDPHC diazonium salt: Investigation of its usability in the determination of phenol and chlorophenols using CV, SWV and DPV techniques

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dc.authorid0000-0002-9447-3065en_US
dc.contributor.authorÇelik, Hacı Hasan
dc.contributor.authorÖzcan, Saniye
dc.contributor.authorMulazimoğlu, Ayşen Demir
dc.contributor.authorYılmaz, Ecir
dc.contributor.authorMercimek, Bedrettin
dc.contributor.authorYılmaz, İbrahim
dc.date.accessioned2020-06-05T12:32:46Z
dc.date.available2020-06-05T12:32:46Z
dc.date.issued2020en_US
dc.departmentKMÜ, Kamil Özdağ Fen Fakültesi, Kimya Bölümüen_US
dc.descriptionWOS:000530085000002en_US
dc.description.abstractElectrochemical and spectroelectrochemical properties of newly synthesized diazonium salt of 2-(2-(1,3-dioxo- 3,3a-dihydro-1H-isoindol-2(7aH)-yl)-1-(3 methyl-3-phenylcyclobutyl)ethylidene) hydrazinecarboxamide (DDPHC-DAS) were studied using glassy carbon (GC) electrode. In the current study, surface characterization was performed by cyclic voltammetry (CV). Besides electrochemical impedance spectroscopy (EIS) was used for the electrochemical and spectroelectrochemical characterization. Surface images were obtained using scanning electron microscopy (SEM). After completion of modification and characterization process, DDPHC-DAS surface was examined for the usability for the quantitative determination of phenol and chlorophenol derivatives by using CV, square wave voltammetry (SWV) and differential pulse voltammetry (DPV). Phenol and chlorophenol solutions that were prepared in Britton-Robinson (BR) buffer solution (pH 8-12) were employed in this research. The presented study proves that all of compounds can be quantitatively determined not only simultaneously but also independently.en_US
dc.identifier.citationÇelik, H. H., Özcan, S., Mülazımoğlu, A. D., Yılmaz, E., Mercimek, B., Çukurovalı, A., Yılmaz, I., ... Mülazımoğlu, I. E. (2020). The synthesis of a novel DDPHC diazonium salt: Investigation of its usability in the determination of phenol and chlorophenols using CV, SWV and DPV techniques. Inorganic Chemistry Communications, 116, 107893.en_US
dc.identifier.doi10.1016/j.inoche.2020.107893
dc.identifier.issn1387-7003
dc.identifier.issn1879-0259
dc.identifier.scopus2-s2.0-85082180286
dc.identifier.scopusqualityQ2
dc.identifier.urihttps://doi.org/10.1016/j.inoche.2020.107893
dc.identifier.urihttps://hdl.handle.net/11492/3500
dc.identifier.volume116en_US
dc.identifier.wosWOS:000530085000002
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Sceince
dc.indekslendigikaynakScopus
dc.institutionauthorYılmaz, İbrahim
dc.language.isoen
dc.publisherElsevier Scienceen_US
dc.relation.journalInorganic Chemistry Communicationsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectDDPHC-DASen_US
dc.subjectCyclic Voltammetryen_US
dc.subjectSquare Wave Voltammetryen_US
dc.subjectDifferential Pulse Voltammetryen_US
dc.subjectChemical Sensor Electrodeen_US
dc.titleThe synthesis of a novel DDPHC diazonium salt: Investigation of its usability in the determination of phenol and chlorophenols using CV, SWV and DPV techniquesen_US
dc.typeArticle

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